BQS Organic Blind Sample Program
Analytes by Multiple Methods
FLUTICASONE PROPIONATE

 Pct Recovery = 116% 
 Schedule Code = 2440  Pct Recovery = 133% 
 Schedule Code = 2440  Pct Recovery = 500% 
 Schedule Code = 2440  Schedule Code = LC9017 
 Minimum Whisker = 11% 
 First Quartile = 43% 
 Median = 58% 
 Third Quartile = 64% 
 Maximum Whisker = 72% 
 Mean = 52% 
 Standard Deviation = 16% 
 Number of Observations = 14  Schedule Code = LC9017 
 Minimum Whisker = 11% 
 First Quartile = 43% 
 Median = 58% 
 Third Quartile = 64% 
 Maximum Whisker = 72% 
 Mean = 52% 
 Standard Deviation = 16% 
 Number of Observations = 14  Schedule Code = LC9017 
 Minimum Whisker = 11% 
 First Quartile = 43% 
 Median = 58% 
 Third Quartile = 64% 
 Maximum Whisker = 72% 
 Mean = 52% 
 Standard Deviation = 16% 
 Number of Observations = 14  Schedule Code = LC9017 
 Minimum Whisker = 11% 
 First Quartile = 43% 
 Median = 58% 
 Third Quartile = 64% 
 Maximum Whisker = 72% 
 Mean = 52% 
 Standard Deviation = 16% 
 Number of Observations = 14  Schedule Code = LC9017 
 Minimum Whisker = 11% 
 First Quartile = 43% 
 Median = 58% 
 Third Quartile = 64% 
 Maximum Whisker = 72% 
 Mean = 52% 
 Standard Deviation = 16% 
 Number of Observations = 14  Schedule Code = LC9017 
 Minimum Whisker = 11% 
 First Quartile = 43% 
 Median = 58% 
 Third Quartile = 64% 
 Maximum Whisker = 72% 
 Mean = 52% 
 Standard Deviation = 16% 
 Number of Observations = 14  Schedule Code = LC9017 
 Minimum Whisker = 11% 
 First Quartile = 43% 
 Median = 58% 
 Third Quartile = 64% 
 Maximum Whisker = 72% 
 Mean = 52% 
 Standard Deviation = 16% 
 Number of Observations = 14  Schedule Code = LC9017 
 Minimum Whisker = 11% 
 First Quartile = 43% 
 Median = 58% 
 Third Quartile = 64% 
 Maximum Whisker = 72% 
 Mean = 52% 
 Standard Deviation = 16% 
 Number of Observations = 14  Schedule Code = LC9017 
 Minimum Whisker = 11% 
 First Quartile = 43% 
 Median = 58% 
 Third Quartile = 64% 
 Maximum Whisker = 72% 
 Mean = 52% 
 Standard Deviation = 16% 
 Number of Observations = 14  Schedule Code = LC9017 
 Minimum Whisker = 11% 
 First Quartile = 43% 
 Median = 58% 
 Third Quartile = 64% 
 Maximum Whisker = 72% 
 Mean = 52% 
 Standard Deviation = 16% 
 Number of Observations = 14  Schedule Code = 2440 
 Minimum Whisker = 17% 
 First Quartile = 53% 
 Median = 66% 
 Third Quartile = 77% 
 Maximum Whisker = 112% 
 Mean = 72% 
 Standard Deviation = 55% 
 Number of Observations = 74  Schedule Code = 2440 
 Minimum Whisker = 17% 
 First Quartile = 53% 
 Median = 66% 
 Third Quartile = 77% 
 Maximum Whisker = 112% 
 Mean = 72% 
 Standard Deviation = 55% 
 Number of Observations = 74  Schedule Code = 2440 
 Minimum Whisker = 17% 
 First Quartile = 53% 
 Median = 66% 
 Third Quartile = 77% 
 Maximum Whisker = 112% 
 Mean = 72% 
 Standard Deviation = 55% 
 Number of Observations = 74  Schedule Code = 2440 
 Minimum Whisker = 17% 
 First Quartile = 53% 
 Median = 66% 
 Third Quartile = 77% 
 Maximum Whisker = 112% 
 Mean = 72% 
 Standard Deviation = 55% 
 Number of Observations = 74  Schedule Code = 2440 
 Minimum Whisker = 17% 
 First Quartile = 53% 
 Median = 66% 
 Third Quartile = 77% 
 Maximum Whisker = 112% 
 Mean = 72% 
 Standard Deviation = 55% 
 Number of Observations = 74  Schedule Code = 2440 
 Minimum Whisker = 17% 
 First Quartile = 53% 
 Median = 66% 
 Third Quartile = 77% 
 Maximum Whisker = 112% 
 Mean = 72% 
 Standard Deviation = 55% 
 Number of Observations = 74  Schedule Code = 2440 
 Minimum Whisker = 17% 
 First Quartile = 53% 
 Median = 66% 
 Third Quartile = 77% 
 Maximum Whisker = 112% 
 Mean = 72% 
 Standard Deviation = 55% 
 Number of Observations = 74  Schedule Code = 2440 
 Minimum Whisker = 17% 
 First Quartile = 53% 
 Median = 66% 
 Third Quartile = 77% 
 Maximum Whisker = 112% 
 Mean = 72% 
 Standard Deviation = 55% 
 Number of Observations = 74  Schedule Code = 2440 
 Minimum Whisker = 17% 
 First Quartile = 53% 
 Median = 66% 
 Third Quartile = 77% 
 Maximum Whisker = 112% 
 Mean = 72% 
 Standard Deviation = 55% 
 Number of Observations = 74  Schedule Code = 2440 
 Minimum Whisker = 17% 
 First Quartile = 53% 
 Median = 66% 
 Third Quartile = 77% 
 Maximum Whisker = 112% 
 Mean = 72% 
 Standard Deviation = 55% 
 Number of Observations = 74  Y = 1
The SGPlot Procedure

BQS Organic Blind Sample Program
Analytes by Multiple Methods
FLUTICASONE PROPIONATE

 spikemix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Expected Conc. = 8.9 
 Lab Value = 3.920 
 reportunit = ng/L  spikemix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Expected Conc. = 17.8 
 Lab Value = 10.800 
 reportunit = ng/L  spikemix = ERA 0507-12-06.1: 40 µl 
 Expected Conc. = 17.8 
 Lab Value = 7.560 
 reportunit = ng/L  spikemix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Expected Conc. = 9 
 Lab Value = 5.760 
 reportunit = ng/L  spikemix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Expected Conc. = 8.9 
 Lab Value = 0.960 
 reportunit = ng/L  spikemix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Expected Conc. = 6.75 
 Lab Value = 4.830 
 reportunit = ng/L  spikemix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Expected Conc. = 8.9 
 Lab Value = 3.800 
 reportunit = ng/L  spikemix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Expected Conc. = 8.9 
 Lab Value = 3.810 
 reportunit = ng/L  spikemix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Expected Conc. = 6.675 
 Lab Value = 2.660 
 reportunit = ng/L  spikemix = Abs 053112: 40 µl 
 Expected Conc. = 18 
 Lab Value = 10.400 
 reportunit = ng/L  spikemix = Abs 071112: 40 µl & ERA 0507-12-06.1: 40 µl 
 Expected Conc. = 17.8 
 Lab Value = 10.500 
 reportunit = ng/L  spikemix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Expected Conc. = 9 
 Lab Value = 5.870 
 reportunit = ng/L  spikemix = Abs 053112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Expected Conc. = 9 
 Lab Value = 5.510 
 reportunit = ng/L  spikemix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Expected Conc. = 9 
 Lab Value = 5.850 
 reportunit = ng/L  spikemix = ERA 06281704: 20 µl & ERA 06281702: 20 µl 
 Expected Conc. = 9.18 
 Lab Value = 4.760 
 reportunit = ng/L  spikemix = ERA 06281704: 50 µl & ERA 06281702: 50 µl 
 Expected Conc. = 22.95 
 Lab Value = 13.100 
 reportunit = ng/L  spikemix = ERA 06281704: 20 µl & Abs 072517Pharm1: 20 µl 
 Expected Conc. = 9.18 
 Lab Value = 5.620 
 reportunit = ng/L  spikemix = ERA 06281703: 20 µl & ERA 06281704: 20 µl 
 Expected Conc. = 9.18 
 Lab Value = 52.200 
 reportunit = ng/L  spikemix = ERA 06281703: 20 µl & Abs 071817Pharm: 20 µl 
 Expected Conc. = 9.2 
 Lab Value = 3.880 
 reportunit = ng/L  spikemix = ERA 06281703: 50 µl & Abs 071817Pharm: 50 µl 
 Expected Conc. = 23 
 Lab Value = 9.110 
 reportunit = ng/L  spikemix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl 
 Expected Conc. = 29.3 
 Lab Value = 20.800 
 reportunit = ng/L  spikemix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl 
 Expected Conc. = 29.3 
 Lab Value = 27.900 
 reportunit = ng/L  spikemix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl 
 Expected Conc. = 11.72 
 Lab Value = 6.420 
 reportunit = ng/L  spikemix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl 
 Expected Conc. = 11.72 
 Lab Value = 7.410 
 reportunit = ng/L  spikemix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl 
 Expected Conc. = 6.88 
 Lab Value = 5.040 
 reportunit = ng/L  spikemix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl 
 Expected Conc. = 6.88 
 Lab Value = 4.780 
 reportunit = ng/L  spikemix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl 
 Expected Conc. = 27.52 
 Lab Value = 14.800 
 reportunit = ng/L  spikemix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl 
 Expected Conc. = 6.88 
 Lab Value = 4.330 
 reportunit = ng/L  spikemix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl 
 Expected Conc. = 13.76 
 Lab Value = 15.400 
 reportunit = ng/L  spikemix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl 
 Expected Conc. = 6.88 
 Lab Value = 1.280 
 reportunit = ng/L  spikemix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl 
 Expected Conc. = 13.76 
 Lab Value = 12.200 
 reportunit = ng/L  spikemix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl 
 Expected Conc. = 13.84 
 Lab Value = 6.480 
 reportunit = ng/L  spikemix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl 
 Expected Conc. = 27.68 
 Lab Value = 11.100 
 reportunit = ng/L  spikemix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl 
 Expected Conc. = 6.92 
 Lab Value = 7.060 
 reportunit = ng/L  spikemix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl 
 Expected Conc. = 18.75 
 Lab Value = 15.600 
 reportunit = ng/L  spikemix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl 
 Expected Conc. = 18.75 
 Lab Value = 16.100 
 reportunit = ng/L  spikemix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl 
 Expected Conc. = 18.15 
 Lab Value = 9.640 
 reportunit = ng/L  spikemix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl 
 Expected Conc. = 18.15 
 Lab Value = 14.800 
 reportunit = ng/L  spikemix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl 
 Expected Conc. = 9.68 
 Lab Value = 4.690 
 reportunit = ng/L  spikemix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl 
 Expected Conc. = 9.375 
 Lab Value = 6.100 
 reportunit = ng/L  spikemix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl 
 Expected Conc. = 10 
 Lab Value = 6.460 
 reportunit = ng/L  spikemix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl 
 Expected Conc. = 18.75 
 Lab Value = 14.500 
 reportunit = ng/L  spikemix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl 
 Expected Conc. = 18.75 
 Lab Value = 12.900 
 reportunit = ng/L  spikemix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl 
 Expected Conc. = 18.75 
 Lab Value = 13.700 
 reportunit = ng/L  spikemix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl 
 Expected Conc. = 18.75 
 Lab Value = 13.100 
 reportunit = ng/L  spikemix = Abs 072517Pharm2: 20 µl & ERA 06281704: 20 µl 
 Expected Conc. = 9.18 
 Lab Value = 5.220 
 reportunit = ng/L  spikemix = Abs 072517Pharm2: 80 µl & Abs 071817Pharm: 80 µl 
 Expected Conc. = 36.8 
 Lab Value = 36.100 
 reportunit = ng/L  spikemix = Abs 072517Pharm2: 50 µl & Abs 071817Pharm: 50 µl 
 Expected Conc. = 23 
 Lab Value = 13.400 
 reportunit = ng/L  spikemix = Abs 072517Pharm1: 50 µl & Abs 071817Pharm: 50 µl 
 Expected Conc. = 23 
 Lab Value = 8.860 
 reportunit = ng/L  spikemix = Abs 071817Pharm: 50 µl & Abs 072517Pharm1: 50 µl 
 Expected Conc. = 23 
 Lab Value = 16.100 
 reportunit = ng/L  spikemix = Abs 071817Pharm: 80 µl & Abs 072517Pharm1: 80 µl 
 Expected Conc. = 36.8 
 Lab Value = 28.100 
 reportunit = ng/L  spikemix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl 
 Expected Conc. = 23.44 
 Lab Value = 11.900 
 reportunit = ng/L  spikemix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl 
 Expected Conc. = 23.44 
 Lab Value = 13.600 
 reportunit = ng/L  spikemix = Abs 061416: 80 µl & Abs 060916PHARM: 80 µl 
 Expected Conc. = 23.44 
 Lab Value = 13.000 
 reportunit = ng/L  spikemix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl 
 Expected Conc. = 11.72 
 Lab Value = 7.150 
 reportunit = ng/L  spikemix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl 
 Expected Conc. = 11.72 
 Lab Value = 6.890 
 reportunit = ng/L  spikemix = Abs 060916PHARM: 20 µl & Abs 071817Pharm: 20 µl 
 Expected Conc. = 15.06 
 Lab Value = 6.880 
 reportunit = ng/L  spikemix = Abs 060916PHARM: 80 µl & Abs 061516PHARM: 80 µl 
 Expected Conc. = 23.44 
 Lab Value = 13.300 
 reportunit = ng/L  spikemix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl 
 Expected Conc. = 23.44 
 Lab Value = 19.500 
 reportunit = ng/L  spikemix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl 
 Expected Conc. = 23.44 
 Lab Value = 16.500 
 reportunit = ng/L  spikemix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl 
 Expected Conc. = 11.72 
 Lab Value = 4.720 
 reportunit = ng/L  spikemix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl 
 Expected Conc. = 11.72 
 Lab Value = 6.210 
 reportunit = ng/L  spikemix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl 
 Expected Conc. = 23.44 
 Lab Value = 18.700 
 reportunit = ng/L  spikemix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl 
 Expected Conc. = 23.44 
 Lab Value = 18.800 
 reportunit = ng/L  spikemix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl 
 Expected Conc. = 6.92 
 Lab Value = 2.880 
 reportunit = ng/L  spikemix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl 
 Expected Conc. = 6.92 
 Lab Value = 3.210 
 reportunit = ng/L  spikemix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl 
 Expected Conc. = 13.84 
 Lab Value = 16.100 
 reportunit = ng/L  spikemix = Abs 052215: 40 µl & Abs 050115: 40 µl 
 Expected Conc. = 13.84 
 Lab Value = 13.400 
 reportunit = ng/L  spikemix = Abs 052215: 80 µl & Abs 050115: 80 µl 
 Expected Conc. = 27.68 
 Lab Value = 19.500 
 reportunit = ng/L  spikemix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl 
 Expected Conc. = 3.44 
 Lab Value = 4.560 
 reportunit = ng/L  spikemix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl 
 Expected Conc. = 27.52 
 Lab Value = 20.800 
 reportunit = ng/L  spikemix = Abs 051315: 20 µl & Abs 052215: 20 µl 
 Expected Conc. = 6.92 
 Lab Value = 5.130 
 reportunit = ng/L  spikemix = Abs 051315: 40 µl & Abs 052215: 40 µl 
 Expected Conc. = 13.84 
 Lab Value = 10.700 
 reportunit = ng/L  spikemix = Abs 051315: 20 µl & Abs 052215: 20 µl 
 Expected Conc. = 6.92 
 Lab Value = 3.730 
 reportunit = ng/L  spikemix = Abs 050115: 20 µl & Abs 052215: 20 µl 
 Expected Conc. = 6.92 
 Lab Value = 4.480 
 reportunit = ng/L  spikemix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl 
 Expected Conc. = 18.75 
 Lab Value = 13.800 
 reportunit = ng/L  spikemix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl 
 Expected Conc. = 10 
 Lab Value = 3.600 
 reportunit = ng/L  spikemix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl 
 Expected Conc. = 9.375 
 Lab Value = 6.210 
 reportunit = ng/L  spikemix = Abs 041814: 30 µl & Abs 041614: 30 µl 
 Expected Conc. = 9.075 
 Lab Value = 4.290 
 reportunit = ng/L  spikemix = Abs 041814: 60 µl & Abs 041614: 60 µl 
 Expected Conc. = 18.15 
 Lab Value = 18.200 
 reportunit = ng/L  spikemix = Abs 041814: 30 µl & Abs 041614: 30 µl 
 Expected Conc. = 9.075 
 Lab Value = 8.390 
 reportunit = ng/L  spikemix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl 
 Expected Conc. = 9.68 
 Lab Value = 1.640 
 reportunit = ng/L  spikemix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl 
 Expected Conc. = 9.68 
 Lab Value = 6.630 
 reportunit = ng/L  spikemix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl 
 Expected Conc. = 18.15 
 Lab Value = 12.300 
 reportunit = ng/L  spikemix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl 
 Expected Conc. = 9.075 
 Lab Value = 3.580 
 reportunit = ng/L  spikemix = Abs 041614: 30 µl & Abs 041714: 30 µl 
 Expected Conc. = 9.075 
 Lab Value = 4.510 
 reportunit = ng/L  spikemix = Abs 041614: 60 µl & Abs 041714: 60 µl 
 Expected Conc. = 18.15 
 Lab Value = 13.600 
 reportunit = ng/L  spikemix = Abs 041614: 30 µl & Abs 041714: 30 µl 
 Expected Conc. = 9.075 
 Lab Value = 9.730 
 reportunit = ng/L  Y = 1
The SGPlot Procedure

BQS Organic Blind Sample Program
Analytes by Multiple Methods
FLUTICASONE PROPIONATE

 spikemix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl 
 Expected Conc. = 8.9 
 Lab Value = 3.920 
 reportunit = ng/L  spikemix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl 
 Expected Conc. = 17.8 
 Lab Value = 10.800 
 reportunit = ng/L  spikemix = ERA 0507-12-06.1: 40 µl 
 Expected Conc. = 17.8 
 Lab Value = 7.560 
 reportunit = ng/L  spikemix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl 
 Expected Conc. = 9 
 Lab Value = 5.760 
 reportunit = ng/L  spikemix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl 
 Expected Conc. = 8.9 
 Lab Value = 0.960 
 reportunit = ng/L  spikemix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl 
 Expected Conc. = 6.75 
 Lab Value = 4.830 
 reportunit = ng/L  spikemix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Expected Conc. = 8.9 
 Lab Value = 3.800 
 reportunit = ng/L  spikemix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl 
 Expected Conc. = 8.9 
 Lab Value = 3.810 
 reportunit = ng/L  spikemix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl 
 Expected Conc. = 6.675 
 Lab Value = 2.660 
 reportunit = ng/L  spikemix = Abs 053112: 40 µl 
 Expected Conc. = 18 
 Lab Value = 10.400 
 reportunit = ng/L  spikemix = Abs 071112: 40 µl & ERA 0507-12-06.1: 40 µl 
 Expected Conc. = 17.8 
 Lab Value = 10.500 
 reportunit = ng/L  spikemix = Abs 071112: 20 µl & Abs 053112: 20 µl 
 Expected Conc. = 9 
 Lab Value = 5.870 
 reportunit = ng/L  spikemix = Abs 053112: 20 µl & ERA 0507-12-06.2: 20 µl 
 Expected Conc. = 9 
 Lab Value = 5.510 
 reportunit = ng/L  spikemix = Abs 053112: 20 µl & Abs 060112: 20 µl 
 Expected Conc. = 9 
 Lab Value = 5.850 
 reportunit = ng/L  spikemix = ERA 06281704: 20 µl & ERA 06281702: 20 µl 
 Expected Conc. = 9.18 
 Lab Value = 4.760 
 reportunit = ng/L  spikemix = ERA 06281704: 50 µl & ERA 06281702: 50 µl 
 Expected Conc. = 22.95 
 Lab Value = 13.100 
 reportunit = ng/L  spikemix = ERA 06281704: 20 µl & Abs 072517Pharm1: 20 µl 
 Expected Conc. = 9.18 
 Lab Value = 5.620 
 reportunit = ng/L  spikemix = ERA 06281703: 20 µl & ERA 06281704: 20 µl 
 Expected Conc. = 9.18 
 Lab Value = 52.200 
 reportunit = ng/L  spikemix = ERA 06281703: 20 µl & Abs 071817Pharm: 20 µl 
 Expected Conc. = 9.2 
 Lab Value = 3.880 
 reportunit = ng/L  spikemix = ERA 06281703: 50 µl & Abs 071817Pharm: 50 µl 
 Expected Conc. = 23 
 Lab Value = 9.110 
 reportunit = ng/L  spikemix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl 
 Expected Conc. = 29.3 
 Lab Value = 20.800 
 reportunit = ng/L  spikemix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl 
 Expected Conc. = 29.3 
 Lab Value = 27.900 
 reportunit = ng/L  spikemix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl 
 Expected Conc. = 11.72 
 Lab Value = 6.420 
 reportunit = ng/L  spikemix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl 
 Expected Conc. = 11.72 
 Lab Value = 7.410 
 reportunit = ng/L  spikemix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl 
 Expected Conc. = 6.88 
 Lab Value = 5.040 
 reportunit = ng/L  spikemix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl 
 Expected Conc. = 6.88 
 Lab Value = 4.780 
 reportunit = ng/L  spikemix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl 
 Expected Conc. = 27.52 
 Lab Value = 14.800 
 reportunit = ng/L  spikemix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl 
 Expected Conc. = 6.88 
 Lab Value = 4.330 
 reportunit = ng/L  spikemix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl 
 Expected Conc. = 13.76 
 Lab Value = 15.400 
 reportunit = ng/L  spikemix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl 
 Expected Conc. = 6.88 
 Lab Value = 1.280 
 reportunit = ng/L  spikemix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl 
 Expected Conc. = 13.76 
 Lab Value = 12.200 
 reportunit = ng/L  spikemix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl 
 Expected Conc. = 13.84 
 Lab Value = 6.480 
 reportunit = ng/L  spikemix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl 
 Expected Conc. = 27.68 
 Lab Value = 11.100 
 reportunit = ng/L  spikemix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl 
 Expected Conc. = 6.92 
 Lab Value = 7.060 
 reportunit = ng/L  spikemix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl 
 Expected Conc. = 18.75 
 Lab Value = 15.600 
 reportunit = ng/L  spikemix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl 
 Expected Conc. = 18.75 
 Lab Value = 16.100 
 reportunit = ng/L  spikemix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl 
 Expected Conc. = 18.15 
 Lab Value = 9.640 
 reportunit = ng/L  spikemix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl 
 Expected Conc. = 18.15 
 Lab Value = 14.800 
 reportunit = ng/L  spikemix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl 
 Expected Conc. = 9.68 
 Lab Value = 4.690 
 reportunit = ng/L  spikemix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl 
 Expected Conc. = 9.375 
 Lab Value = 6.100 
 reportunit = ng/L  spikemix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl 
 Expected Conc. = 10 
 Lab Value = 6.460 
 reportunit = ng/L  spikemix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl 
 Expected Conc. = 18.75 
 Lab Value = 14.500 
 reportunit = ng/L  spikemix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl 
 Expected Conc. = 18.75 
 Lab Value = 12.900 
 reportunit = ng/L  spikemix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl 
 Expected Conc. = 18.75 
 Lab Value = 13.700 
 reportunit = ng/L  spikemix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl 
 Expected Conc. = 18.75 
 Lab Value = 13.100 
 reportunit = ng/L  spikemix = Abs 072517Pharm2: 20 µl & ERA 06281704: 20 µl 
 Expected Conc. = 9.18 
 Lab Value = 5.220 
 reportunit = ng/L  spikemix = Abs 072517Pharm2: 80 µl & Abs 071817Pharm: 80 µl 
 Expected Conc. = 36.8 
 Lab Value = 36.100 
 reportunit = ng/L  spikemix = Abs 072517Pharm2: 50 µl & Abs 071817Pharm: 50 µl 
 Expected Conc. = 23 
 Lab Value = 13.400 
 reportunit = ng/L  spikemix = Abs 072517Pharm1: 50 µl & Abs 071817Pharm: 50 µl 
 Expected Conc. = 23 
 Lab Value = 8.860 
 reportunit = ng/L  spikemix = Abs 071817Pharm: 50 µl & Abs 072517Pharm1: 50 µl 
 Expected Conc. = 23 
 Lab Value = 16.100 
 reportunit = ng/L  spikemix = Abs 071817Pharm: 80 µl & Abs 072517Pharm1: 80 µl 
 Expected Conc. = 36.8 
 Lab Value = 28.100 
 reportunit = ng/L  spikemix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl 
 Expected Conc. = 23.44 
 Lab Value = 11.900 
 reportunit = ng/L  spikemix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl 
 Expected Conc. = 23.44 
 Lab Value = 13.600 
 reportunit = ng/L  spikemix = Abs 061416: 80 µl & Abs 060916PHARM: 80 µl 
 Expected Conc. = 23.44 
 Lab Value = 13.000 
 reportunit = ng/L  spikemix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl 
 Expected Conc. = 11.72 
 Lab Value = 7.150 
 reportunit = ng/L  spikemix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl 
 Expected Conc. = 11.72 
 Lab Value = 6.890 
 reportunit = ng/L  spikemix = Abs 060916PHARM: 20 µl & Abs 071817Pharm: 20 µl 
 Expected Conc. = 15.06 
 Lab Value = 6.880 
 reportunit = ng/L  spikemix = Abs 060916PHARM: 80 µl & Abs 061516PHARM: 80 µl 
 Expected Conc. = 23.44 
 Lab Value = 13.300 
 reportunit = ng/L  spikemix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl 
 Expected Conc. = 23.44 
 Lab Value = 19.500 
 reportunit = ng/L  spikemix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl 
 Expected Conc. = 23.44 
 Lab Value = 16.500 
 reportunit = ng/L  spikemix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl 
 Expected Conc. = 11.72 
 Lab Value = 4.720 
 reportunit = ng/L  spikemix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl 
 Expected Conc. = 11.72 
 Lab Value = 6.210 
 reportunit = ng/L  spikemix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl 
 Expected Conc. = 23.44 
 Lab Value = 18.700 
 reportunit = ng/L  spikemix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl 
 Expected Conc. = 23.44 
 Lab Value = 18.800 
 reportunit = ng/L  spikemix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl 
 Expected Conc. = 6.92 
 Lab Value = 2.880 
 reportunit = ng/L  spikemix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl 
 Expected Conc. = 6.92 
 Lab Value = 3.210 
 reportunit = ng/L  spikemix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl 
 Expected Conc. = 13.84 
 Lab Value = 16.100 
 reportunit = ng/L  spikemix = Abs 052215: 40 µl & Abs 050115: 40 µl 
 Expected Conc. = 13.84 
 Lab Value = 13.400 
 reportunit = ng/L  spikemix = Abs 052215: 80 µl & Abs 050115: 80 µl 
 Expected Conc. = 27.68 
 Lab Value = 19.500 
 reportunit = ng/L  spikemix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl 
 Expected Conc. = 3.44 
 Lab Value = 4.560 
 reportunit = ng/L  spikemix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl 
 Expected Conc. = 27.52 
 Lab Value = 20.800 
 reportunit = ng/L  spikemix = Abs 051315: 20 µl & Abs 052215: 20 µl 
 Expected Conc. = 6.92 
 Lab Value = 5.130 
 reportunit = ng/L  spikemix = Abs 051315: 40 µl & Abs 052215: 40 µl 
 Expected Conc. = 13.84 
 Lab Value = 10.700 
 reportunit = ng/L  spikemix = Abs 051315: 20 µl & Abs 052215: 20 µl 
 Expected Conc. = 6.92 
 Lab Value = 3.730 
 reportunit = ng/L  spikemix = Abs 050115: 20 µl & Abs 052215: 20 µl 
 Expected Conc. = 6.92 
 Lab Value = 4.480 
 reportunit = ng/L  spikemix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl 
 Expected Conc. = 18.75 
 Lab Value = 13.800 
 reportunit = ng/L  spikemix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl 
 Expected Conc. = 10 
 Lab Value = 3.600 
 reportunit = ng/L  spikemix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl 
 Expected Conc. = 9.375 
 Lab Value = 6.210 
 reportunit = ng/L  spikemix = Abs 041814: 30 µl & Abs 041614: 30 µl 
 Expected Conc. = 9.075 
 Lab Value = 4.290 
 reportunit = ng/L  spikemix = Abs 041814: 60 µl & Abs 041614: 60 µl 
 Expected Conc. = 18.15 
 Lab Value = 18.200 
 reportunit = ng/L  spikemix = Abs 041814: 30 µl & Abs 041614: 30 µl 
 Expected Conc. = 9.075 
 Lab Value = 8.390 
 reportunit = ng/L  spikemix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl 
 Expected Conc. = 9.68 
 Lab Value = 1.640 
 reportunit = ng/L  spikemix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl 
 Expected Conc. = 9.68 
 Lab Value = 6.630 
 reportunit = ng/L  spikemix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl 
 Expected Conc. = 18.15 
 Lab Value = 12.300 
 reportunit = ng/L  spikemix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl 
 Expected Conc. = 9.075 
 Lab Value = 3.580 
 reportunit = ng/L  spikemix = Abs 041614: 30 µl & Abs 041714: 30 µl 
 Expected Conc. = 9.075 
 Lab Value = 4.510 
 reportunit = ng/L  spikemix = Abs 041614: 60 µl & Abs 041714: 60 µl 
 Expected Conc. = 18.15 
 Lab Value = 13.600 
 reportunit = ng/L  spikemix = Abs 041614: 30 µl & Abs 041714: 30 µl 
 Expected Conc. = 9.075 
 Lab Value = 9.730 
 reportunit = ng/L  Y = 1
The SGPlot Procedure