BQS Organic Blind Sample Program
Analytes by Multiple Methods
FLUTICASONE PROPIONATE

Pct Recovery = 116% Schedule Code = 2440 Pct Recovery = 133% Schedule Code = 2440 Pct Recovery = 500% Schedule Code = 2440 Schedule Code = LC9017 Minimum Whisker = 11% First Quartile = 43% Median = 58% Third Quartile = 64% Maximum Whisker = 72% Mean = 52% Standard Deviation = 16% Number of Observations = 14 Schedule Code = LC9017 Minimum Whisker = 11% First Quartile = 43% Median = 58% Third Quartile = 64% Maximum Whisker = 72% Mean = 52% Standard Deviation = 16% Number of Observations = 14 Schedule Code = LC9017 Minimum Whisker = 11% First Quartile = 43% Median = 58% Third Quartile = 64% Maximum Whisker = 72% Mean = 52% Standard Deviation = 16% Number of Observations = 14 Schedule Code = LC9017 Minimum Whisker = 11% First Quartile = 43% Median = 58% Third Quartile = 64% Maximum Whisker = 72% Mean = 52% Standard Deviation = 16% Number of Observations = 14 Schedule Code = LC9017 Minimum Whisker = 11% First Quartile = 43% Median = 58% Third Quartile = 64% Maximum Whisker = 72% Mean = 52% Standard Deviation = 16% Number of Observations = 14 Schedule Code = LC9017 Minimum Whisker = 11% First Quartile = 43% Median = 58% Third Quartile = 64% Maximum Whisker = 72% Mean = 52% Standard Deviation = 16% Number of Observations = 14 Schedule Code = LC9017 Minimum Whisker = 11% First Quartile = 43% Median = 58% Third Quartile = 64% Maximum Whisker = 72% Mean = 52% Standard Deviation = 16% Number of Observations = 14 Schedule Code = LC9017 Minimum Whisker = 11% First Quartile = 43% Median = 58% Third Quartile = 64% Maximum Whisker = 72% Mean = 52% Standard Deviation = 16% Number of Observations = 14 Schedule Code = LC9017 Minimum Whisker = 11% First Quartile = 43% Median = 58% Third Quartile = 64% Maximum Whisker = 72% Mean = 52% Standard Deviation = 16% Number of Observations = 14 Schedule Code = LC9017 Minimum Whisker = 11% First Quartile = 43% Median = 58% Third Quartile = 64% Maximum Whisker = 72% Mean = 52% Standard Deviation = 16% Number of Observations = 14 Schedule Code = 2440 Minimum Whisker = 17% First Quartile = 53% Median = 66% Third Quartile = 77% Maximum Whisker = 112% Mean = 72% Standard Deviation = 55% Number of Observations = 74 Schedule Code = 2440 Minimum Whisker = 17% First Quartile = 53% Median = 66% Third Quartile = 77% Maximum Whisker = 112% Mean = 72% Standard Deviation = 55% Number of Observations = 74 Schedule Code = 2440 Minimum Whisker = 17% First Quartile = 53% Median = 66% Third Quartile = 77% Maximum Whisker = 112% Mean = 72% Standard Deviation = 55% Number of Observations = 74 Schedule Code = 2440 Minimum Whisker = 17% First Quartile = 53% Median = 66% Third Quartile = 77% Maximum Whisker = 112% Mean = 72% Standard Deviation = 55% Number of Observations = 74 Schedule Code = 2440 Minimum Whisker = 17% First Quartile = 53% Median = 66% Third Quartile = 77% Maximum Whisker = 112% Mean = 72% Standard Deviation = 55% Number of Observations = 74 Schedule Code = 2440 Minimum Whisker = 17% First Quartile = 53% Median = 66% Third Quartile = 77% Maximum Whisker = 112% Mean = 72% Standard Deviation = 55% Number of Observations = 74 Schedule Code = 2440 Minimum Whisker = 17% First Quartile = 53% Median = 66% Third Quartile = 77% Maximum Whisker = 112% Mean = 72% Standard Deviation = 55% Number of Observations = 74 Schedule Code = 2440 Minimum Whisker = 17% First Quartile = 53% Median = 66% Third Quartile = 77% Maximum Whisker = 112% Mean = 72% Standard Deviation = 55% Number of Observations = 74 Schedule Code = 2440 Minimum Whisker = 17% First Quartile = 53% Median = 66% Third Quartile = 77% Maximum Whisker = 112% Mean = 72% Standard Deviation = 55% Number of Observations = 74 Schedule Code = 2440 Minimum Whisker = 17% First Quartile = 53% Median = 66% Third Quartile = 77% Maximum Whisker = 112% Mean = 72% Standard Deviation = 55% Number of Observations = 74 Y = 1
The SGPlot Procedure

BQS Organic Blind Sample Program
Analytes by Multiple Methods
FLUTICASONE PROPIONATE

spikemix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl Expected Conc. = 8.9 Lab Value = 3.920 reportunit = ng/L spikemix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl Expected Conc. = 17.8 Lab Value = 10.800 reportunit = ng/L spikemix = ERA 0507-12-06.1: 40 µl Expected Conc. = 17.8 Lab Value = 7.560 reportunit = ng/L spikemix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl Expected Conc. = 9 Lab Value = 5.760 reportunit = ng/L spikemix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl Expected Conc. = 8.9 Lab Value = 0.960 reportunit = ng/L spikemix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl Expected Conc. = 6.75 Lab Value = 4.830 reportunit = ng/L spikemix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl Expected Conc. = 8.9 Lab Value = 3.800 reportunit = ng/L spikemix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl Expected Conc. = 8.9 Lab Value = 3.810 reportunit = ng/L spikemix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl Expected Conc. = 6.675 Lab Value = 2.660 reportunit = ng/L spikemix = Abs 053112: 40 µl Expected Conc. = 18 Lab Value = 10.400 reportunit = ng/L spikemix = Abs 071112: 40 µl & ERA 0507-12-06.1: 40 µl Expected Conc. = 17.8 Lab Value = 10.500 reportunit = ng/L spikemix = Abs 071112: 20 µl & Abs 053112: 20 µl Expected Conc. = 9 Lab Value = 5.870 reportunit = ng/L spikemix = Abs 053112: 20 µl & ERA 0507-12-06.2: 20 µl Expected Conc. = 9 Lab Value = 5.510 reportunit = ng/L spikemix = Abs 053112: 20 µl & Abs 060112: 20 µl Expected Conc. = 9 Lab Value = 5.850 reportunit = ng/L spikemix = ERA 06281704: 20 µl & ERA 06281702: 20 µl Expected Conc. = 9.18 Lab Value = 4.760 reportunit = ng/L spikemix = ERA 06281704: 50 µl & ERA 06281702: 50 µl Expected Conc. = 22.95 Lab Value = 13.100 reportunit = ng/L spikemix = ERA 06281704: 20 µl & Abs 072517Pharm1: 20 µl Expected Conc. = 9.18 Lab Value = 5.620 reportunit = ng/L spikemix = ERA 06281703: 20 µl & ERA 06281704: 20 µl Expected Conc. = 9.18 Lab Value = 52.200 reportunit = ng/L spikemix = ERA 06281703: 20 µl & Abs 071817Pharm: 20 µl Expected Conc. = 9.2 Lab Value = 3.880 reportunit = ng/L spikemix = ERA 06281703: 50 µl & Abs 071817Pharm: 50 µl Expected Conc. = 23 Lab Value = 9.110 reportunit = ng/L spikemix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Expected Conc. = 29.3 Lab Value = 20.800 reportunit = ng/L spikemix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Expected Conc. = 29.3 Lab Value = 27.900 reportunit = ng/L spikemix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Expected Conc. = 11.72 Lab Value = 6.420 reportunit = ng/L spikemix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Expected Conc. = 11.72 Lab Value = 7.410 reportunit = ng/L spikemix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Expected Conc. = 6.88 Lab Value = 5.040 reportunit = ng/L spikemix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Expected Conc. = 6.88 Lab Value = 4.780 reportunit = ng/L spikemix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Expected Conc. = 27.52 Lab Value = 14.800 reportunit = ng/L spikemix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Expected Conc. = 6.88 Lab Value = 4.330 reportunit = ng/L spikemix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Expected Conc. = 13.76 Lab Value = 15.400 reportunit = ng/L spikemix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Expected Conc. = 6.88 Lab Value = 1.280 reportunit = ng/L spikemix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Expected Conc. = 13.76 Lab Value = 12.200 reportunit = ng/L spikemix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Expected Conc. = 13.84 Lab Value = 6.480 reportunit = ng/L spikemix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Expected Conc. = 27.68 Lab Value = 11.100 reportunit = ng/L spikemix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Expected Conc. = 6.92 Lab Value = 7.060 reportunit = ng/L spikemix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Expected Conc. = 18.75 Lab Value = 15.600 reportunit = ng/L spikemix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Expected Conc. = 18.75 Lab Value = 16.100 reportunit = ng/L spikemix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Expected Conc. = 18.15 Lab Value = 9.640 reportunit = ng/L spikemix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Expected Conc. = 18.15 Lab Value = 14.800 reportunit = ng/L spikemix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Expected Conc. = 9.68 Lab Value = 4.690 reportunit = ng/L spikemix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Expected Conc. = 9.375 Lab Value = 6.100 reportunit = ng/L spikemix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Expected Conc. = 10 Lab Value = 6.460 reportunit = ng/L spikemix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Expected Conc. = 18.75 Lab Value = 14.500 reportunit = ng/L spikemix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Expected Conc. = 18.75 Lab Value = 12.900 reportunit = ng/L spikemix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Expected Conc. = 18.75 Lab Value = 13.700 reportunit = ng/L spikemix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Expected Conc. = 18.75 Lab Value = 13.100 reportunit = ng/L spikemix = Abs 072517Pharm2: 20 µl & ERA 06281704: 20 µl Expected Conc. = 9.18 Lab Value = 5.220 reportunit = ng/L spikemix = Abs 072517Pharm2: 80 µl & Abs 071817Pharm: 80 µl Expected Conc. = 36.8 Lab Value = 36.100 reportunit = ng/L spikemix = Abs 072517Pharm2: 50 µl & Abs 071817Pharm: 50 µl Expected Conc. = 23 Lab Value = 13.400 reportunit = ng/L spikemix = Abs 072517Pharm1: 50 µl & Abs 071817Pharm: 50 µl Expected Conc. = 23 Lab Value = 8.860 reportunit = ng/L spikemix = Abs 071817Pharm: 50 µl & Abs 072517Pharm1: 50 µl Expected Conc. = 23 Lab Value = 16.100 reportunit = ng/L spikemix = Abs 071817Pharm: 80 µl & Abs 072517Pharm1: 80 µl Expected Conc. = 36.8 Lab Value = 28.100 reportunit = ng/L spikemix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Expected Conc. = 23.44 Lab Value = 11.900 reportunit = ng/L spikemix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Expected Conc. = 23.44 Lab Value = 13.600 reportunit = ng/L spikemix = Abs 061416: 80 µl & Abs 060916PHARM: 80 µl Expected Conc. = 23.44 Lab Value = 13.000 reportunit = ng/L spikemix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Expected Conc. = 11.72 Lab Value = 7.150 reportunit = ng/L spikemix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Expected Conc. = 11.72 Lab Value = 6.890 reportunit = ng/L spikemix = Abs 060916PHARM: 20 µl & Abs 071817Pharm: 20 µl Expected Conc. = 15.06 Lab Value = 6.880 reportunit = ng/L spikemix = Abs 060916PHARM: 80 µl & Abs 061516PHARM: 80 µl Expected Conc. = 23.44 Lab Value = 13.300 reportunit = ng/L spikemix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Expected Conc. = 23.44 Lab Value = 19.500 reportunit = ng/L spikemix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Expected Conc. = 23.44 Lab Value = 16.500 reportunit = ng/L spikemix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Expected Conc. = 11.72 Lab Value = 4.720 reportunit = ng/L spikemix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Expected Conc. = 11.72 Lab Value = 6.210 reportunit = ng/L spikemix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Expected Conc. = 23.44 Lab Value = 18.700 reportunit = ng/L spikemix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Expected Conc. = 23.44 Lab Value = 18.800 reportunit = ng/L spikemix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Expected Conc. = 6.92 Lab Value = 2.880 reportunit = ng/L spikemix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Expected Conc. = 6.92 Lab Value = 3.210 reportunit = ng/L spikemix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Expected Conc. = 13.84 Lab Value = 16.100 reportunit = ng/L spikemix = Abs 052215: 40 µl & Abs 050115: 40 µl Expected Conc. = 13.84 Lab Value = 13.400 reportunit = ng/L spikemix = Abs 052215: 80 µl & Abs 050115: 80 µl Expected Conc. = 27.68 Lab Value = 19.500 reportunit = ng/L spikemix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Expected Conc. = 3.44 Lab Value = 4.560 reportunit = ng/L spikemix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Expected Conc. = 27.52 Lab Value = 20.800 reportunit = ng/L spikemix = Abs 051315: 20 µl & Abs 052215: 20 µl Expected Conc. = 6.92 Lab Value = 5.130 reportunit = ng/L spikemix = Abs 051315: 40 µl & Abs 052215: 40 µl Expected Conc. = 13.84 Lab Value = 10.700 reportunit = ng/L spikemix = Abs 051315: 20 µl & Abs 052215: 20 µl Expected Conc. = 6.92 Lab Value = 3.730 reportunit = ng/L spikemix = Abs 050115: 20 µl & Abs 052215: 20 µl Expected Conc. = 6.92 Lab Value = 4.480 reportunit = ng/L spikemix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Expected Conc. = 18.75 Lab Value = 13.800 reportunit = ng/L spikemix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Expected Conc. = 10 Lab Value = 3.600 reportunit = ng/L spikemix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Expected Conc. = 9.375 Lab Value = 6.210 reportunit = ng/L spikemix = Abs 041814: 30 µl & Abs 041614: 30 µl Expected Conc. = 9.075 Lab Value = 4.290 reportunit = ng/L spikemix = Abs 041814: 60 µl & Abs 041614: 60 µl Expected Conc. = 18.15 Lab Value = 18.200 reportunit = ng/L spikemix = Abs 041814: 30 µl & Abs 041614: 30 µl Expected Conc. = 9.075 Lab Value = 8.390 reportunit = ng/L spikemix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Expected Conc. = 9.68 Lab Value = 1.640 reportunit = ng/L spikemix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Expected Conc. = 9.68 Lab Value = 6.630 reportunit = ng/L spikemix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Expected Conc. = 18.15 Lab Value = 12.300 reportunit = ng/L spikemix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Expected Conc. = 9.075 Lab Value = 3.580 reportunit = ng/L spikemix = Abs 041614: 30 µl & Abs 041714: 30 µl Expected Conc. = 9.075 Lab Value = 4.510 reportunit = ng/L spikemix = Abs 041614: 60 µl & Abs 041714: 60 µl Expected Conc. = 18.15 Lab Value = 13.600 reportunit = ng/L spikemix = Abs 041614: 30 µl & Abs 041714: 30 µl Expected Conc. = 9.075 Lab Value = 9.730 reportunit = ng/L Y = 1
The SGPlot Procedure

BQS Organic Blind Sample Program
Analytes by Multiple Methods
FLUTICASONE PROPIONATE

spikemix = Spex Organics T1120802015: 20 µl & ERA 0507-12-06.1: 20 µl Expected Conc. = 8.9 Lab Value = 3.920 reportunit = ng/L spikemix = Spex Organics T1120802015: 40 µl & ERA 0507-12-06.1: 40 µl Expected Conc. = 17.8 Lab Value = 10.800 reportunit = ng/L spikemix = ERA 0507-12-06.1: 40 µl Expected Conc. = 17.8 Lab Value = 7.560 reportunit = ng/L spikemix = ERA 0823-11-05.2: 20 µl & Abs 053112: 20 µl Expected Conc. = 9 Lab Value = 5.760 reportunit = ng/L spikemix = ERA 0823-11-05.1: 20 µl & ERA 0507-12-06.1: 20 µl Expected Conc. = 8.9 Lab Value = 0.960 reportunit = ng/L spikemix = ERA 0823-11-05.1: 15 µl & Abs 053112: 15 µl Expected Conc. = 6.75 Lab Value = 4.830 reportunit = ng/L spikemix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl Expected Conc. = 8.9 Lab Value = 3.800 reportunit = ng/L spikemix = ERA 0507-12-06.1: 20 µl & ERA 0507-12-06.2: 20 µl Expected Conc. = 8.9 Lab Value = 3.810 reportunit = ng/L spikemix = ERA 0507-12-06.1: 15 µl & Abs 060112: 15 µl Expected Conc. = 6.675 Lab Value = 2.660 reportunit = ng/L spikemix = Abs 053112: 40 µl Expected Conc. = 18 Lab Value = 10.400 reportunit = ng/L spikemix = Abs 071112: 40 µl & ERA 0507-12-06.1: 40 µl Expected Conc. = 17.8 Lab Value = 10.500 reportunit = ng/L spikemix = Abs 071112: 20 µl & Abs 053112: 20 µl Expected Conc. = 9 Lab Value = 5.870 reportunit = ng/L spikemix = Abs 053112: 20 µl & ERA 0507-12-06.2: 20 µl Expected Conc. = 9 Lab Value = 5.510 reportunit = ng/L spikemix = Abs 053112: 20 µl & Abs 060112: 20 µl Expected Conc. = 9 Lab Value = 5.850 reportunit = ng/L spikemix = ERA 06281704: 20 µl & ERA 06281702: 20 µl Expected Conc. = 9.18 Lab Value = 4.760 reportunit = ng/L spikemix = ERA 06281704: 50 µl & ERA 06281702: 50 µl Expected Conc. = 22.95 Lab Value = 13.100 reportunit = ng/L spikemix = ERA 06281704: 20 µl & Abs 072517Pharm1: 20 µl Expected Conc. = 9.18 Lab Value = 5.620 reportunit = ng/L spikemix = ERA 06281703: 20 µl & ERA 06281704: 20 µl Expected Conc. = 9.18 Lab Value = 52.200 reportunit = ng/L spikemix = ERA 06281703: 20 µl & Abs 071817Pharm: 20 µl Expected Conc. = 9.2 Lab Value = 3.880 reportunit = ng/L spikemix = ERA 06281703: 50 µl & Abs 071817Pharm: 50 µl Expected Conc. = 23 Lab Value = 9.110 reportunit = ng/L spikemix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Expected Conc. = 29.3 Lab Value = 20.800 reportunit = ng/L spikemix = ERA 04281603: 100 µl & Abs 060916PHARM: 100 µl Expected Conc. = 29.3 Lab Value = 27.900 reportunit = ng/L spikemix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Expected Conc. = 11.72 Lab Value = 6.420 reportunit = ng/L spikemix = ERA 04281603: 40 µl & Abs 060916PHARM: 40 µl Expected Conc. = 11.72 Lab Value = 7.410 reportunit = ng/L spikemix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Expected Conc. = 6.88 Lab Value = 5.040 reportunit = ng/L spikemix = ERA 0406-15-09: 20 µl & ERA 0406-15-07A: 20 µl Expected Conc. = 6.88 Lab Value = 4.780 reportunit = ng/L spikemix = ERA 0406-15-09: 80 µl & ERA 0406-15-07A: 80 µl Expected Conc. = 27.52 Lab Value = 14.800 reportunit = ng/L spikemix = ERA 0406-15-09: 20 µl & Abs 050115: 20 µl Expected Conc. = 6.88 Lab Value = 4.330 reportunit = ng/L spikemix = ERA 0406-15-09: 40 µl & Abs 050115: 40 µl Expected Conc. = 13.76 Lab Value = 15.400 reportunit = ng/L spikemix = ERA 0406-15-08: 20 µl & ERA 0406-15-09: 20 µl Expected Conc. = 6.88 Lab Value = 1.280 reportunit = ng/L spikemix = ERA 0406-15-08: 40 µl & ERA 0406-15-09: 40 µl Expected Conc. = 13.76 Lab Value = 12.200 reportunit = ng/L spikemix = ERA 0406-15-08: 40 µl & Abs 052215: 40 µl Expected Conc. = 13.84 Lab Value = 6.480 reportunit = ng/L spikemix = ERA 0406-15-08: 80 µl & Abs 052215: 80 µl Expected Conc. = 27.68 Lab Value = 11.100 reportunit = ng/L spikemix = ERA 0406-15-08: 20 µl & Abs 052215: 20 µl Expected Conc. = 6.92 Lab Value = 7.060 reportunit = ng/L spikemix = ERA 0319-14-05: 15 µl & ERA 0318-14-02: 15 µl Expected Conc. = 18.75 Lab Value = 15.600 reportunit = ng/L spikemix = ERA 0319-14-05: 60 µl & ERA 0318-14-02: 60 µl Expected Conc. = 18.75 Lab Value = 16.100 reportunit = ng/L spikemix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Expected Conc. = 18.15 Lab Value = 9.640 reportunit = ng/L spikemix = ERA 0319-14-05: 15 µl & Abs 041614: 15 µl Expected Conc. = 18.15 Lab Value = 14.800 reportunit = ng/L spikemix = ERA 0319-14-05: 8 µl & Abs 041614: 8 µl Expected Conc. = 9.68 Lab Value = 4.690 reportunit = ng/L spikemix = ERA 0318-14-02: 30 µl & ERA 0319-14-05: 30 µl Expected Conc. = 9.375 Lab Value = 6.100 reportunit = ng/L spikemix = ERA 0318-14-02: 8 µl & ERA 0319-14-04: 8 µl Expected Conc. = 10 Lab Value = 6.460 reportunit = ng/L spikemix = ERA 0318-14-02: 15 µl & ERA 0319-14-04: 15 µl Expected Conc. = 18.75 Lab Value = 14.500 reportunit = ng/L spikemix = ERA 0318-14-02: 60 µl & ERA 0319-14-04: 60 µl Expected Conc. = 18.75 Lab Value = 12.900 reportunit = ng/L spikemix = ERA 0318-14-02: 15 µl & Abs 041714: 15 µl Expected Conc. = 18.75 Lab Value = 13.700 reportunit = ng/L spikemix = ERA 0318-14-02: 60 µl & Abs 041714: 60 µl Expected Conc. = 18.75 Lab Value = 13.100 reportunit = ng/L spikemix = Abs 072517Pharm2: 20 µl & ERA 06281704: 20 µl Expected Conc. = 9.18 Lab Value = 5.220 reportunit = ng/L spikemix = Abs 072517Pharm2: 80 µl & Abs 071817Pharm: 80 µl Expected Conc. = 36.8 Lab Value = 36.100 reportunit = ng/L spikemix = Abs 072517Pharm2: 50 µl & Abs 071817Pharm: 50 µl Expected Conc. = 23 Lab Value = 13.400 reportunit = ng/L spikemix = Abs 072517Pharm1: 50 µl & Abs 071817Pharm: 50 µl Expected Conc. = 23 Lab Value = 8.860 reportunit = ng/L spikemix = Abs 071817Pharm: 50 µl & Abs 072517Pharm1: 50 µl Expected Conc. = 23 Lab Value = 16.100 reportunit = ng/L spikemix = Abs 071817Pharm: 80 µl & Abs 072517Pharm1: 80 µl Expected Conc. = 36.8 Lab Value = 28.100 reportunit = ng/L spikemix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Expected Conc. = 23.44 Lab Value = 11.900 reportunit = ng/L spikemix = Abs 061516PHARM: 80 µl & Abs 060916PHARM: 80 µl Expected Conc. = 23.44 Lab Value = 13.600 reportunit = ng/L spikemix = Abs 061416: 80 µl & Abs 060916PHARM: 80 µl Expected Conc. = 23.44 Lab Value = 13.000 reportunit = ng/L spikemix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Expected Conc. = 11.72 Lab Value = 7.150 reportunit = ng/L spikemix = Abs 060916PHARM: 40 µl & ERA 04281604: 40 µl Expected Conc. = 11.72 Lab Value = 6.890 reportunit = ng/L spikemix = Abs 060916PHARM: 20 µl & Abs 071817Pharm: 20 µl Expected Conc. = 15.06 Lab Value = 6.880 reportunit = ng/L spikemix = Abs 060916PHARM: 80 µl & Abs 061516PHARM: 80 µl Expected Conc. = 23.44 Lab Value = 13.300 reportunit = ng/L spikemix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Expected Conc. = 23.44 Lab Value = 19.500 reportunit = ng/L spikemix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Expected Conc. = 23.44 Lab Value = 16.500 reportunit = ng/L spikemix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Expected Conc. = 11.72 Lab Value = 4.720 reportunit = ng/L spikemix = Abs 060916PHARM: 40 µl & Abs 061416: 40 µl Expected Conc. = 11.72 Lab Value = 6.210 reportunit = ng/L spikemix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Expected Conc. = 23.44 Lab Value = 18.700 reportunit = ng/L spikemix = Abs 060916PHARM: 80 µl & Abs 061416: 80 µl Expected Conc. = 23.44 Lab Value = 18.800 reportunit = ng/L spikemix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Expected Conc. = 6.92 Lab Value = 2.880 reportunit = ng/L spikemix = Abs 052215: 20 µl & ERA 0406-15-07A: 20 µl Expected Conc. = 6.92 Lab Value = 3.210 reportunit = ng/L spikemix = Abs 052215: 40 µl & ERA 0406-15-07A: 40 µl Expected Conc. = 13.84 Lab Value = 16.100 reportunit = ng/L spikemix = Abs 052215: 40 µl & Abs 050115: 40 µl Expected Conc. = 13.84 Lab Value = 13.400 reportunit = ng/L spikemix = Abs 052215: 80 µl & Abs 050115: 80 µl Expected Conc. = 27.68 Lab Value = 19.500 reportunit = ng/L spikemix = Abs 051315: 10 µl & ERA 0406-15-09: 10 µl Expected Conc. = 3.44 Lab Value = 4.560 reportunit = ng/L spikemix = Abs 051315: 80 µl & ERA 0406-15-09: 80 µl Expected Conc. = 27.52 Lab Value = 20.800 reportunit = ng/L spikemix = Abs 051315: 20 µl & Abs 052215: 20 µl Expected Conc. = 6.92 Lab Value = 5.130 reportunit = ng/L spikemix = Abs 051315: 40 µl & Abs 052215: 40 µl Expected Conc. = 13.84 Lab Value = 10.700 reportunit = ng/L spikemix = Abs 051315: 20 µl & Abs 052215: 20 µl Expected Conc. = 6.92 Lab Value = 3.730 reportunit = ng/L spikemix = Abs 050115: 20 µl & Abs 052215: 20 µl Expected Conc. = 6.92 Lab Value = 4.480 reportunit = ng/L spikemix = Abs 041814: 15 µl & ERA 0318-14-02: 15 µl Expected Conc. = 18.75 Lab Value = 13.800 reportunit = ng/L spikemix = Abs 041814: 8 µl & ERA 0318-14-02: 8 µl Expected Conc. = 10 Lab Value = 3.600 reportunit = ng/L spikemix = Abs 041814: 30 µl & ERA 0318-14-02: 30 µl Expected Conc. = 9.375 Lab Value = 6.210 reportunit = ng/L spikemix = Abs 041814: 30 µl & Abs 041614: 30 µl Expected Conc. = 9.075 Lab Value = 4.290 reportunit = ng/L spikemix = Abs 041814: 60 µl & Abs 041614: 60 µl Expected Conc. = 18.15 Lab Value = 18.200 reportunit = ng/L spikemix = Abs 041814: 30 µl & Abs 041614: 30 µl Expected Conc. = 9.075 Lab Value = 8.390 reportunit = ng/L spikemix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Expected Conc. = 9.68 Lab Value = 1.640 reportunit = ng/L spikemix = Abs 041614: 8 µl & ERA 0319-14-04: 8 µl Expected Conc. = 9.68 Lab Value = 6.630 reportunit = ng/L spikemix = Abs 041614: 15 µl & ERA 0319-14-04: 15 µl Expected Conc. = 18.15 Lab Value = 12.300 reportunit = ng/L spikemix = Abs 041614: 30 µl & ERA 0319-14-04: 30 µl Expected Conc. = 9.075 Lab Value = 3.580 reportunit = ng/L spikemix = Abs 041614: 30 µl & Abs 041714: 30 µl Expected Conc. = 9.075 Lab Value = 4.510 reportunit = ng/L spikemix = Abs 041614: 60 µl & Abs 041714: 60 µl Expected Conc. = 18.15 Lab Value = 13.600 reportunit = ng/L spikemix = Abs 041614: 30 µl & Abs 041714: 30 µl Expected Conc. = 9.075 Lab Value = 9.730 reportunit = ng/L Y = 1
The SGPlot Procedure